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Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquidchromatographytandem mass spectrometry

WEI Yimei,ZHANG Yuan,XU Jian,GUO Changsheng,LI Lei,FAN Wenhong

Frontiers of Environmental Science & Engineering 2014, Volume 8, Issue 3,   Pages 357-371 doi: 10.1007/s11783-013-0580-6

Abstract: Sediment samples were solvent-extracted, followed by tandem SPE (strong anion exchange (SAX) + HLB) clean-upsLiquid chromatographytandem mass spectrometry (LC-MS/MS) with multiple reaction monitoring (MRM) detection

Keywords: antibiotics     liquid chromatographytandem mass spectrometry (LC-MS/MS)     water     sediment     fish muscle    

Perfluorocarboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs) in surface and tap water around Lake Taihu in China

Yong QIU, He JING, Hanchang SHI,

Frontiers of Environmental Science & Engineering 2010, Volume 4, Issue 3,   Pages 301-310 doi: 10.1007/s11783-010-0236-8

Abstract: Perfluorinated compounds (PFCs) are ubiquitously distributed in the environment mainly as perfluoro-carboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs). In this paper, six PFCAs and two PFASs were quantified in surface and tap water samples from 12 sites around Lake Taihu near Shanghai City in East China. Predominant PFCs were perfluorooctanoic acid (PFOA) and perfluorooctane sulfonate (PFOS), of which the concentration ranges were 6.8–206 and 1.2–45 ng·L, the geometric means were 35.3 and 9.4 ng·L, and the median (quartile range) values were 31.4 (34.4) and 10.4 (10.7) ng·L, respectively. Other PFCs were also detected but in much lower concentrations than PFOA. The sources of the PFCs were expected to be direct industrial discharges in the Lake Taihu area, and this area was also a possible source of PFCs contaminations in Shanghai district in the downstream. PFCs distributions were found different in the upstream, downstream and north part of Lake Taihu. Occurrences of PFCs in the tap water in Lake Taihu area indicated their exposure to the local people. A brief estimation of the environmental risks by PFCs implied no acute or immediate risks from PFCs to local human health, but chronic risks from PFOA in the tap water should be considered in the downstream regions.

Keywords: perfluorocarboxylic acids (PFCAs)     perfluoroalkyl sulfonates (PFASs)     Lake Taihu area     ultra performance liquidchromatography with tandem mass spectrometry (UPLC-MS)    

An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal

Feng Zhu, Zhijian Yao, Wenliang Ji, Deye Liu, Hao Zhang, Aimin Li, Zongli Huo, Qing Zhou

Frontiers of Environmental Science & Engineering 2020, Volume 14, Issue 3, doi: 10.1007/s11783-020-1228-y

Abstract: Detection limits of method (SPE-UPLC-MS/MS) ranged between 0.03 and 0.6 ng/L. 22 PPCPs were determinedSPE with home-made hydrophilic polymeric sorbent followed by ultra-performance liquid chromatographyand tandem mass spectrometry was validated, and the method achieved good linearity (r2>0.991, for all

Keywords: Hydrophilic resin     Solid phase extraction     Pharmaceuticals and personal care product     Ultra-performance liquidchromatography and tandem mass spectrometry     Environmental water    

Trace analysis of off-flavor/odor compounds in water using liquid-liquid microextraction coupled withgas chromatography—positive chemical ionization-tandem mass spectrometry

Jian LU,Paul S. WILLS,P. CHRIS WILSON

Frontiers of Environmental Science & Engineering 2016, Volume 10, Issue 3,   Pages 477-481 doi: 10.1007/s11783-015-0820-z

Abstract: friendly method was developed for analysis of off-flavor/odor compounds in fresh and salt water using gas chromatographywith chemical ionization-tandem mass spectrometry.

Keywords: off-flavor/odor compounds     liquid-liquid microextraction     gas chromatography-tandem mass spectrometry    

Simultaneous analysis of five taste and odor compounds in surface water using solid-phase extraction and gas chromatography-massspectrometry

Wenfeng SUN, Ruibao JIA, Baoyu GAO

Frontiers of Environmental Science & Engineering 2012, Volume 6, Issue 1,   Pages 66-74 doi: 10.1007/s11783-010-0257-3

Abstract: In this paper, a method using solid-phase extraction (SPE) and gas chromatography-mass spectrometry (GC-MS) was developed to simultaneously analyze five taste and odor compounds in surface water, i.e.,The mass spectrometry was operated in selective ion monitoring (SIM) mode.

Keywords: solid-phase extraction (SPE)     gas chromatography-mass spectrometry (GC-MS)     taste and odor compounds     surface    

Perfluoroalkane acids in human milk under the global monitoring plan of the Stockholm Convention on Persistent Organic Pollutants (2008–2019)

Frontiers of Environmental Science & Engineering 2022, Volume 16, Issue 10, doi: 10.1007/s11783-022-1541-8

Abstract:

● Perfluorooctanesulfonic acid and perfluorooctanoic acid highest in human milk.

Keywords: Human biomonitoring     Human breast milk     LC-MS/MS analysis     Lifestyle parameters    

Detecting

Chengkun WANG, Xiaojian ZHANG, Jun WANG, Chao CHEN

Frontiers of Environmental Science & Engineering 2012, Volume 6, Issue 6,   Pages 770-777 doi: 10.1007/s11783-012-0412-0

Abstract: An ultra-performance liquid chromatography-tandem mass spectrometry method with solid phase extractionThe solid phase extraction procedures including pH, enrichment process and MS/MS parameters including

Keywords: N-nitrosamines     water treatment plant     distribution system     ultra-performance liquid chromatography-tandemmass spectrometry    

Determination of persistent organic pollutants by gas chromatography/laser multiphoton ionization/time-of-flightmass spectrometry

Osamu SHITAMICHI, Taiki MATSUI, Yamei HUI, Weiwei CHEN, Totaro IMASAKA

Frontiers of Environmental Science & Engineering 2012, Volume 6, Issue 1,   Pages 26-31 doi: 10.1007/s11783-011-0374-7

Abstract: capillary column, since the retention time was reduced and the amount of analytes introduced into the massAs demonstrated, a technique involving laser multiphoton ionization/time-of-flight mass spectrometry

Keywords: biphenyls (PCBs)     polycyclic aromatic hydrocarbons (PAHs)     laser multiphoton ionization/time-of-flight massspectrometry (MPI/TOF-MS)    

Photocatalytic degradation of methyl orange using ZnO/TiO composites

Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,

Frontiers of Environmental Science & Engineering 2009, Volume 3, Issue 3,   Pages 271-280 doi: 10.1007/s11783-009-0035-2

Abstract: A sample analysis was conducted using liquid chromatography coupled with electrospray ionization ion-trapmass spectrometry.

Keywords: photocatalytic degradation     methyl orange     ZnO/TiO2 composites     high performance liquid chromatographymass spectrometry (HPLC-MS)    

Characteristics and removal mechanism of the precursors of N-chloro-2,2-dichloroacetamide in a drinking water treatment process at Taihu Lake

Frontiers of Environmental Science & Engineering 2021, Volume 15, Issue 5, doi: 10.1007/s11783-020-1338-6

Abstract:

• N-Cl-DCAM, an emerging N-DBP in drinking water was investigated.

Keywords: N-chloro-2     2-dichloroacetamide     Liquid chromatography with tandem mass spectrometry     Precursors     Removal    

Determination of 27 pharmaceuticals and personal care products (PPCPs) in water: The benefit of isotope dilution

Xueqi Fan, Jie Gao, Wenchao Li, Jun Huang, Gang Yu

Frontiers of Environmental Science & Engineering 2020, Volume 14, Issue 1, doi: 10.1007/s11783-019-1187-3

Abstract: samples were extracted by solid phase extraction (SPE), and determined by isotope dilution method using liquidchromatography coupled to tandem triple quadruple mass spectrometer (LC-MS/MS).

Keywords: personal care products (PPCPs)     Isotopically labeled standard (ILSs)     Water     Solid-phase extraction (SPE)     LC-MS/MS    

LC/MS/MS and radioisotope method combined for recognizing the affinity between catalpol and OCT2 transporter

Zhiyu ZHANG, Changxiao LIU, Duanyun SI, Rong LU, Xiulin YI

Frontiers of Chemical Science and Engineering 2012, Volume 6, Issue 4,   Pages 436-442 doi: 10.1007/s11705-012-1222-4

Abstract: In this paper, chromatography/tandem mass spectrometry (LC/MS/MS) combined with radioisotope method wasAnd samples were precipitated with methanol and quantified with LC/MS/MS.

Keywords: catalpol     LC/MS/MS     OCT2    

Pyrolysis behaviors of oil sludge based on TG/FTIR and PY-GC/MS

Wei SONG, Jianguo LIU, Yongfeng NIE,

Frontiers of Environmental Science & Engineering 2010, Volume 4, Issue 1,   Pages 59-64 doi: 10.1007/s11783-009-0152-y

Abstract: Thermogravimetric Analysis-Fourier Transform Infrared Spectroscopy and Pyrolysis-Gas Chromatography/MassSpectrometry were employed to investigate the pyrolysis process and products of oil sludge.useful not only for the proper design of a pyrolysis system, but also for improving the utilization of liquid

Keywords: pyrolysis     Thermogravimetric Analysis-Fourier Transform Infrared Spectroscopy (TG-FTIR)     Pyrolysis-Gas Chromatography/Mass Spectrometry (PY-GC/MS)    

Analysis of Brucella cellular fatty acids

Zhen-Xiang ZHAO MS, Hai JIANG MD, Bu-Yun CUI MS, Hong-Yan ZHAO, Dong-Ri PIAO MS, Lan-Yu LI, Su-Zhen HAOMS,

Frontiers of Medicine 2010, Volume 4, Issue 2,   Pages 216-219 doi: 10.1007/s11684-010-0037-2

Abstract: were harvested, saponificated, methylated and extracted to provide fatty acid methylesters for gas chromatography

Keywords: Brucella     gas chromatography     cellular fatty acids     dendrogram     typing    

Preparation, identification, and clinical application of anti-HBs monoclonal antibody that binds both wild-type and immune escape mutant HBsAgs

Fanghe LI BM , Chunyan ZHANG MS , Jinghua LIU MS , Xiaoyan ZHANG MS , Bing YAN , Bo ZHANG MS , YongguoHUANG MS , Jingsong GONG BM , Yan CHEN BM ,

Frontiers of Medicine 2009, Volume 3, Issue 3,   Pages 277-283 doi: 10.1007/s11684-009-0047-0

Abstract: Using a standard cellular fusion technique and indirect enzyme-linked immunosorbent assay (ELISA), a hybridoma cell line strain secreting anti-HBs monoclonal antibody (mAb) (defined G6 mAb) was obtained. The cells grew and secreted mAb stably. Antibody titers in the culture supernatant and ascites were 2.048×10 and 4.096×10, respectively. By applying the anti-HBs G6 mAb and horseradish peroxidase (HRP)-labeled goat anti-HBs antibody, we developed a sandwich ELISA (defined G6m ELISA) for detecting both wild-type and immune escape mutant HBsAgs (IEM HBsAg). The assay was performed to detect 17 species of genome recombinant expression HBsAg, including two wild-type species and 15 IEM HBsAg species, which varied in the “a” determinant, in a group of patients infected with hepatitis B virus (HBV). The patients previously had a lower ELISA detection signal [(absorbance of patients/absorbance of normal people (P/N): 1.0―4.5)]. The results demonstrated that the sensitivity of this assay to wild-type HBsAg was no less than 0.125g/L; 12 of 15 IEM HBsAg species (P/N≥2.5) were positive for G6 mAb. Of the positive IEM HBsAg species, two had a low absorbance value at 450nm (), one had an intermediate value and nine had a high value, which was 7.55%(mean), 59.4% and 92.1%―109.4% of the wild-type value, respectively. The two species with low value and the three negative species mutated at the bases 120―124 in the first loop of the HBV “a” determinant. Using the G6 ELISA and two commercial ELISA kits (A and B), 177 patients were tested. The G6 ELISA had a significantly higher detection rate than either commercial ELISAs (19.21% 14.89% and 6.21%, respectively; <0.01, <0.05, respectively).

Keywords: hepatitis B virus     gene variation     hepatitis B surface antigen     immune escape     enzyme-linked immunosorbent assay    

Title Author Date Type Operation

Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquidchromatographytandem mass spectrometry

WEI Yimei,ZHANG Yuan,XU Jian,GUO Changsheng,LI Lei,FAN Wenhong

Journal Article

Perfluorocarboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs) in surface and tap water around Lake Taihu in China

Yong QIU, He JING, Hanchang SHI,

Journal Article

An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal

Feng Zhu, Zhijian Yao, Wenliang Ji, Deye Liu, Hao Zhang, Aimin Li, Zongli Huo, Qing Zhou

Journal Article

Trace analysis of off-flavor/odor compounds in water using liquid-liquid microextraction coupled withgas chromatography—positive chemical ionization-tandem mass spectrometry

Jian LU,Paul S. WILLS,P. CHRIS WILSON

Journal Article

Simultaneous analysis of five taste and odor compounds in surface water using solid-phase extraction and gas chromatography-massspectrometry

Wenfeng SUN, Ruibao JIA, Baoyu GAO

Journal Article

Perfluoroalkane acids in human milk under the global monitoring plan of the Stockholm Convention on Persistent Organic Pollutants (2008–2019)

Journal Article

Detecting

Chengkun WANG, Xiaojian ZHANG, Jun WANG, Chao CHEN

Journal Article

Determination of persistent organic pollutants by gas chromatography/laser multiphoton ionization/time-of-flightmass spectrometry

Osamu SHITAMICHI, Taiki MATSUI, Yamei HUI, Weiwei CHEN, Totaro IMASAKA

Journal Article

Photocatalytic degradation of methyl orange using ZnO/TiO composites

Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,

Journal Article

Characteristics and removal mechanism of the precursors of N-chloro-2,2-dichloroacetamide in a drinking water treatment process at Taihu Lake

Journal Article

Determination of 27 pharmaceuticals and personal care products (PPCPs) in water: The benefit of isotope dilution

Xueqi Fan, Jie Gao, Wenchao Li, Jun Huang, Gang Yu

Journal Article

LC/MS/MS and radioisotope method combined for recognizing the affinity between catalpol and OCT2 transporter

Zhiyu ZHANG, Changxiao LIU, Duanyun SI, Rong LU, Xiulin YI

Journal Article

Pyrolysis behaviors of oil sludge based on TG/FTIR and PY-GC/MS

Wei SONG, Jianguo LIU, Yongfeng NIE,

Journal Article

Analysis of Brucella cellular fatty acids

Zhen-Xiang ZHAO MS, Hai JIANG MD, Bu-Yun CUI MS, Hong-Yan ZHAO, Dong-Ri PIAO MS, Lan-Yu LI, Su-Zhen HAOMS,

Journal Article

Preparation, identification, and clinical application of anti-HBs monoclonal antibody that binds both wild-type and immune escape mutant HBsAgs

Fanghe LI BM , Chunyan ZHANG MS , Jinghua LIU MS , Xiaoyan ZHANG MS , Bing YAN , Bo ZHANG MS , YongguoHUANG MS , Jingsong GONG BM , Yan CHEN BM ,

Journal Article